degrees) for the reflection list as defined for m = 1. This is the recommended format for
the deposition of reflection data with the PDB, and is also the format required for the
An actal file
#
# h,k,l, Fo-squared, sigma(Fo-squared), Fc and phi(calc)
#
data_ta36
_shelx_title ' ta36 in P-1'
_shelx_refln_list_code 6
_shelx_F_calc_maximum 147.61
_exptl_crystal_F_000 628.00
_reflns_d_resolution_high 0.7205
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
_cell_length_a 10.9827
_cell_length_b 11.4038
_cell_length_c 12.1961
_cell_angle_alpha 65.918
_cell_angle_beta 73.507
_cell_angle_gamma 76.655
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_F_calc
_refln_phase_calc
1 0 0 548.13 8.13 23.91 0.0
2 0 0 713.05 6.90 27.04 0.0
3 0 0 4487.70 36.52 61.90 0.0
4 0 0 5185.71 41.46 70.98 0.0
And the relevant part of the corresponding SHELX ins file
TITL ta36 in P-1
CELL 0.71073 10.9827 11.4038 12.1961 65.918 73.507 76.655
ZERR 1.00 0.0005 0.0006 0.0006 0.003 0.003 0.003
LATT 1
SFAC C H N O F S Cu
UNIT 52 45 9 8 6 2 2
WGHT 0.000000
FVAR 0.66533 0.53147
CU1 7 -0.011240 0.599643 0.665074 11.00000 0.02325 0.03784 =
0.02594 -0.00922 -0.00439 -0.00980
O1 4 0.323760 0.794114 0.628981 11.00000 0.02076 0.03749 =
0.07654 -0.03652 -0.01288 -0.00180